Application of the response surface method in optimizing the thickness and hardness of vanadium carbide coatings created by the electrolytic plasma method

Document Type : Research Paper

Authors

1 Assistant Professor, Department of Materials Engineering, Karaj Branch, Islamic Azad University, Karaj, Iran

2 Material Department, Phd studeny, Semnan University, Semnan, Iran

Abstract

One of the new methods of coating coatings is the use of electrolytic plasma method. In the present study, we try to use an electrolytic plasma method of vanadium carbide coating on the surface of the specimen and, in the next step, optimize the effective parameters in making these coatings. In this regard, the RMS test method was used to optimize the coating. The electrolyte is composed of materials such as vanadium oxide, chloride, and NaOH. That NaOH is considered as a conductive enhancer as an important parameter. In addition to NaOH, the difference in voltage and cooking time are also the most important parameters affecting the coating properties, which in this study are considered as independent variables. The dependent variables of the research can also be indicated by thickness and hardness. The results of the study show that the optimum state of the vanadium carbide sample produced by the electrolytic plasma method is 100 V, the NaOH content is about 50 g / l and the duration is 6.65 minutes. The optimum specimen has a hardness of about 1250 Vickers and a thickness of about 29.5 microns.

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References:
1-B.Ghorbanian, & S. M. M.Khoie, (2016). Formation of vanadium carbide with the plasma electrolytic saturation method (PES) and comparison with Thermo Reactive diffusion method (TRD). Acta Metallurgica Slovaca, 22(2), 111-119.
2-B.Ghorbanian, S. M. M., Khoie & M. Rasouli, (2016). INVESTIGATION OF THE ELECTROLYTE EFFECT ON VN CREATED VIA PES. Acta Metallurgica Slovaca, 22(4), 238-248.           
3-Ghorbanian, Babak, et al. "Investigation Of The Electrolyte Effects On Formation Of Vanadium Carbide Via Plasma Electrolytic Saturation Method (Pes)." Surface Review and Letters 23.04 (2016): 1650021.
4-D.J. Blackwood, K.H.W. Seah, Electrochemical cathodic deposition of hydroxy-apatite: Improvements in adhesion and crystallinity, Materials Science and Engineering C 29 (2009) 1233.   
5-W. Simka, M. Kaczmarek, A. Baron-Wieche´c, G. Nawrat, J. Marciniak, J. Zak, Electropolishing and passivation of NiTi shape memory alloy, Electrochimica Acta 55 (2010) 2437.  
6-C.S. Lin, M.T. Chen, J.H. Liu, Structural evolution and adhesion of titanium oxide film containing phosphorus and calcium on titanium by anodic oxidation, Journal of Biomedical Materials Research Part A 85A (2008) 378.
7-H.J. Song, S.H. Park, S.H. Jeong, Y.J. Park, Surface characteristics and bioactivity of oxide films formed by anodic spark oxidation on titanium in different electrolytes, Journal of Materials Processing Technology 209 (2009) 864.
8-M. Long, H.J. Rack, Titanium alloys in total joint replacement—a materials science perspective, Biomaterials 19 (1998) 1621.
9-Momeni, Fariba, et al. "Study of Current and Voltage Diagram In The Formed Vanadium Carbide Coatings Via Plasma Electrolytic Saturation Method." JOURNAL OF MATERIALS 7.11 (2016): 4073-4078.
10-M. Geetha, A.K. Singh, R. Asokamani, A.K. Gogia, Ti based biomaterials, the ultimate choice for orthopedic implants—a review, Progress in Materials Science54 (2009) 397.    
11-Khuri, André I., and Siuli Mukhopadhyay. "Response surface methodology." Wiley Interdisciplinary Reviews: Computational Statistics 2.2 (2010): 128-149.          
12-Carley, Kathleen M., Natalia Y. Kamneva, and Jeff Reminga. Response surface methodology. No. CMU-ISRI-04-136. CARNEGIE-MELLON UNIV PITTSBURGH PA SCHOOL OF COMPUTER SCIENCE, 2004.       
13-Dean, Angela, Daniel Voss, and Danel Draguljić. "Response surface methodology." Design and analysis of experiments. Springer, Cham, 2017. 565-614.
14-Gunst, Richard F. "Response surface methodology: process and product optimization using designed experiments." (1996): 284-286.          
15-Bezerra, Marcos Almeida, et al. "Response surface methodology (RSM) as a tool for optimization in analytical chemistry." Talanta 76.5 (2008): 965-977.
16-Kleijnen, Jack PC. "Response surface methodology." Handbook of simulation optimization. Springer, New York, NY, 2015. 81-104.     
17-Barton, Russell R. "Response surface methodology." Encyclopedia of Operations Research and Management Science. Springer, Boston, MA, 2013. 1307-1313.